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Electron Microscopy Sciences

Technical Data Sheets

Calibration and Installation Procedures for Lanthanum Hexaboride (LaB6) and Cerium Hexaboride (CeB6) Cathodes

EMS Catalog #80920 - 80933

Calibration Procedure for LaB6 or CeBix Cathode

Use the following proposed calibration procedure for correct initial filament current when using an APTech LaB6 or CeBix cathode.

  1. Bypass vacuum interlocks, disable high voltage.
  2. Place load resistor across filament leads in gun chamber with an ammeter in line. Load resistor should be equal to the resistance of the cathode at 1800K (0.67 Ω, 15 watts, 1%*).
  3. Probe transformer primary inputs outside HV tank on circuit boards.
  4. Ramp up primary voltage with filament control knob until cathode’s 1800 K current is obtained on ammeter (2.81 amps). Read primary voltage (V1800). This is the only calibration point that will be useful, as the resistance of the cathode will change with temperature due to changes in the resistivity of the pyrolytic graphite heater blocks.
  5. Install cathode, restore interlocks, pump down.
  6. Ramp cathode slowly to primary V = V1800, ideally with HV set as low as system will allow. Initial resistance of the cathode will be somewhat high due to oxidation of block-to-crystal interfaces. Do not try to saturate or locate beam at this point. Let the cathode sit at V1800 for ~ 3 hrs to remove oxide and stabilize resistance.
  7. Assume that at this point the resistance of the cathode is actually 0.67 Ω and stable, and the filament current is as expected (2.81 amps).
  8. Proceed with saturation procedures. Find correct bias setting to saturate beam without having to increase the primary voltage beyond V1800. The recommended point for maximum brightness is just short of saturation. Align beam, etc
  9. Expect that brightness should be different than seen initially with the CeBix cathode, primarily due to a lower temperature. (Assuming here that the CeBix cathode was initially running hotter than 1800 K).

*Allied Electronics 2005 catalog p. 1160. Stock #’s 524-6002, 524-6005, 524-6010, and 524-6015.

Installation Procedure for CeBix Cathode

Use the following procedure when installing a CeBix cathode in a self biased or an independently biased system.

If you have Self Biased System and are installing a CeBixTM cathode, you must:

  • Increase the distance between the tip of the crystal and the Wehnelt cap. For example, when installing a cathode in a JEOL JBX‐5DII Lithography system, the crystal truncation should be recessed from the front surface of the Wehnelt 3/5 a turn for LaB6, or ¾ turn for CeBix™. Use a similar tip distance relationship when installing CeBix™ in other LaB6 instruments.

-OR-

  • Increase the bias resistance by a factor of 2.

NOTE: In some cases you will need to perform a combination of both of the above.

If you have an Independently Biased System and are installing a CeBixTM cathode, you must:

  • Simply operate it the same way as you would operate a LaB6 cathode. Do expect, however, the total emission current to be approximately half of that obtained when operating a LaB6 cathode.

Online Ordering

Lanthanum Hexaboride (LaB6) and Cerium Hexaboride (CeB6) Cathodes are available online from the EMS Catalog. For ordering or product information, click here.