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Rotary-Pumped Carbon and Sputter Coating System
Q150R Plus Rotary Pumped Coater
The Q150R Plus is suitable for use with Tungsten/LaB6 SEM and Benchtop SEM.
Typical uses
Sputter coating of noble metals using the Q150R S Plus & Q150R ES Plus
Recommended for magnifications:
- Up to x 50k using Au, Au/Pd
- Up to x 100k using Pt (optional)
Carbon cord coating for elemental analysis using the Q150R S Plus & Q150R ES Plus.
Key Features
- Capable of achieving vacuum of 2 x 10-3 mbar
- New touch and swipe capacitive screen
- USB port for upgrades and download of log files
- Multiple-user profiles can be set up on one machine
- New software sorts recipes per user, according to recent use
- 16GB of memory can store more than 1000 recipes
- New multi-color LED visual status indicator
- Interchangeable stage options and plug-in heads
Product Description
The Q150R Plus is available in three configurations:
- Q150R S Plus – An automatic sputter coater for non-oxidizing metals. Available sputtering targets including gold, gold/palladium and platinum.
- Q150R E Plus – An automatic carbon cord coater for SEM applications such as EDS and WDS.
- Q150R ES Plus – A combined system system capable of both sputtering and carbon coating. The deposition heads can be swapped in seconds.
Recommended applications for Q150R Plus
- Low and medium magnifications
- SE signal boost (1 nm or less)
- Table-top SEM coating
- Elemental analysis
- Copper metallization layers
These products are for Research Use Only.
Improved interface
- Capacitive touch screen is more sensitive for ease of use
- User interface software has been extensively revised, using a modern smartphone-style interface
- Comprehensive context-sensitive help screen
- USB interface allows easy software updates and backing up/copying of recipe files to USB stick
- Process log files can be exported via USB port in .csv format for analysis in Excel or similar. Log files include date, time and process parameters.
- 16GB of flash memory can store more than 1000 recipes
- Dual-core ARM processor for a fast, responsive display
Allows multiple users to input and store coating recipes, with a new feature to sort recipes per user according to recent use.
Intelligent system logic automatically detects which insert is in place and displays the appropriate operating settings and controls for that process.
System prompts user to confirm target material and it then automatically selects appropriate parameters for that material.
Intuitive software allows the most inexperienced or occasional operator to rapidly enter and store their own process data. For convenience a number of typical sputtering and carbon coating profiles are already stored but also allows the user to create their own.
Software detects failure to achieve vacuum in a set period of time and shuts down the process in case of vacuum leak, which ensures pump protection from overheating.
Automatic, controlled pulsed carbon cord evaporation
The carbon evaporation process can be terminated using the optional film thickness monitor, which incorporates a quartz crystal monitor, fitted as standard on E and ES models. This recipe ensures that carbon is evaporated in short controlled pulses, which has two effects: protecting the sample from heating and ensuring the accuracy of the film thickness monitor. Pulsing also significantly reduces the amount of debris (including large carbon fragments) associated with traditional carbon "flash" evaporation. Pulsed and ramped carbon rod recipes are supplied as standard.
Cool Magnetron Sputtering
Sputter coating is a technique widely used in various applications; it is possible to create a plasma and sputter metals with high voltage, poor vacuum and no automation. However, this is not suitable for electron microscopy applications because it will heat the sample and can result in damage when the plasma interacts with the sample. The Q 150R Plus series uses low temperature enhanced-plasma magnetrons optimized for the rotary pump pressures, combined with low current and deposition control, which ensures your sample is protected and uniformly coated.
The Q150R S Plus and Q150R ES Plus use easy-change, 57 mm diameter, disc-style targets which are designed to sputter non-oxidizing (noble) metals – ideal for W-SEM applications. The Q150R S Plus and Q150R ES Plus are fitted as standard with a gold (Au) sputter target.
Other targets options include Au/Pd, Pt/Pd, Pd, and Cu. Platinum (Pt) can also be sputtered with the optional Pt coating vacuum hose assembly.
Interchangeable Plug-in Heads
This allows the user to configure the system as a sputter coater, evaporator or glow discharge system – all in one space saving format. A carbon cord evaporation insert is available as an option. Automatic detection of the head type when changed.
Detachable chamber with built-in implosion guard
Removable glass chamber and easily accessible base and top plate allows for an easy cleaning process.
Users can rapidly change the chamber, if necessary, to avoid cross contamination of sensitive samples.
Tall chamber option is available for carbon evaporation to avoid sample heating, to improve uniformity for sputtering and to hold taller samples.
Multiple stage options
The Q150R Plus has specimen stages to meet most requirements. All are easy-change, drop-in style (no screws) and are height adjustable (except for the rotary planetary stage). Some examples:
- Rotation stage (supplied as standard): 50 mm Ø can accommodate six standard stubs. Height can be preset.
- Rotate-tilt stage for improved uniform coating: 50 mm Ø. Tilt and height can be preset.
- Variable angle, rotary planetary stage for heavily contoured samples
- Large flat rotation stage with offset gear box for 4"/100 mm wafers
- Rotation stage for glass microscope slides
Other options are available on request.
Safety
The Q150R Plus meets key industry CE standards:
- All electronic components are protected by covers
- Implosion guard prevents user injury in event of chamber failure
- Vacuum interlocks remove power from deposition sources to prevent user exposure to high voltage in event of chamber being opened
- Electrical interlocks remove power when source head cover opened
- Overheating protection shuts down power supply
Specifications
Instrument Case | 585 mm W x 470 mm D x 410 mm H Total height with coating head open is 650 mm |
Weight | 28.4 kg (Packed 42 kg) |
Packed dimensions | 725 mm W x 660 mm D x 680 mm H |
Work Chamber | Borosilicate glass 150 mm ID x 127 mm H |
Display | 115.5 mm W x 86.4 mm H (active area), 640 RGB x 480 (display format), capacitive touch color display |
User Interface | Full graphical interface with touch screen buttons. Includes features such as a log of the last 1000 coatings and reminders for when maintenance is due. |
Sputter Target | Disc-style 57 mm Ø 0.1 mm thick gold (Au) target is fitted as standard. R S and R ES versions only |
Specimen Stage | 50 mm Ø rotation stage with rotation speed of 8-20 rpm. Other stages available on request. |
Vacuum
Rotary pump | Optional 5 m3/hr two-stage rotary pump with oil mist filter (order separately) |
Vacuum measurement | Pirani gauge |
Ultimate vacuum | 2 x 10-2 mbar Typical ultimate vacuum of the pumping system in a clean instrument after pre-pumping with dry nitrogen gas |
Sputter vacuum range | Between 7 x 10-3 and 1 x 10-1 mbar for gold |
Processes
Sputtering | Sputter current 0-80 mA to a predetermined thickness (with optional FTM) or by the built-in timer. The maximum sputtering time is 60 minutes (without breaking vacuum and with automatically built-in cooling periods). |
Carbon evaporation | A robust, ripple free DC power supply featuring pulse evaporation ensures reproducible carbon evaporation from cord sources. Current pulse: 1-70 A current. |
Visual status indicator
A large multi-color status indicator light provides a visual indication of the state of the equipment, allowing users to easily identify the status of a progress at a distance.
The indicator LED shows the following states:
- Initialization
- Process running
- Idle
- Coating in progress
- Process completed
- Process ended in fault condition
Audio indication also sounds on completion of the process.
Ordering Information
Q150R S Plus
4500 | Q150R S Plus Fully automatic, capacitive touch-screen controlled rotary-pumped sputter coater with status LED indicator. Including quick-release sputter insert, one 57 mm diameter x 0.1 mm gold target, and 50 mm diameter rotating specimen stage. |
POR | Quote |
Q150R E Plus
4503 | Q150R E Plus Fully automatic, capacitive touch-screen controlled rotary pumped carbon fiber evaporation coater with status LED indicator. Including quick-release carbon fiber insert for evaporation of carbon cord, carbon fiber cord, and 50 mm diameter rotating specimen stage. | POR | Quote |
Q150R ES Plus
4507 | Q150R ES Plus Fully automatic, capacitive touch-screen controlled rotary pumped sputter coater and carbon evaporator with status LED indicator. Including quick release sputter insert, one 57 mm diameter x 0.1 mm gold target, and carbon fiber evaporation coater, including quick-release carbon fiber insert for evaporation of carbon cord*, and 50 mm diameter rotating specimen stage. *Coating inserts are interchangeable and can be swapped in seconds. The intelligent system logic automatically recognizes which insert is in place and displays the appropriate operating settings. |
POR | Quote |
Options and Accessories
Rotary pump requirements – order separately
91003 | 5m3 hr two-stage Pfeiffer Duo 6 rotary pump with oil mist filter | 3,100.00 | Add to Cart |
Head inserts and glow discharge
4511 | Additional sputter insert for quick metal change (R E and R ES only). Note: this is an entire sputtering assembly – individual noble metal targets can also be purchased | POR | Quote |
4512 | Carbon rod evaporation insert for 3.05 mm Ø rods (R E and R ES only). Includes manual rod shaper and 3.05 mm Ø carbon rod | POR | Quote |
4513 | Glow discharge insert to modify surface properties (e.g. hydrophobic to hydrophilic conversion) or to clean surface residues (R S and R ES only). Can be retrofitted | POR | Quote |
4514 | Additional standard glass chamber assembly | POR | Quote |
4515 | Extended height vacuum chamber (214 mm high – the standard chamber is 127 mm high). For increased source to sample distance and for coating large specimens | POR | Quote |
4516 | Rotating vacuum spigot allows more convenient connection of the vacuum hose to the rear of the Q150R Plus when bench depth is limited | POR | Quote |
4517 | Film thickness monitor (FTM) attachment. Consists of a built in chamber mounted quartz crystal oscillator (includes crystal). As sputtered or evaporated material is deposited onto the crystal, so its frequency of oscillation is modified. This "modification" is used to measure and control the thickness of material deposited | POR | Quote |
4518 | Spare quartz crystal | 105.00 | Add to Cart |
13530 | Standard coating shield assembly | POR | Quote |
11880 | Extended height coating shield assembly | POR | Quote |
1371 | Platinum coating vacuum hose assembly | POR | Quote |
Specimen stages
All rotating stages have variable rotation of between 8 and 20 rpm.4519 | 50 mm Ø rotate-tilt specimen stage with adjustable tilt (up to 90 degrees) and height (37 mm-60 mm). Has six stub positions for 15 mm or 6.5 mm or ⅛" pin stubs. Stage rotation speed variable between 8 and 20rpm | POR | Quote |
4520 | 90 mm Ø rotating specimen stage for glass microscope slides (up to two x 75 mm x 25 mm slides). Stage rotation speed variable between 8 and 20rpm | POR | Quote |
4521 | Variable angle "Rotacota" rotary planetary stage with 50 mm Ø specimen platform. Has six stub positions for 15 mm or 6.5 mm or ⅛" pin stubs. Stage rotation speed variable between 8 and 20rpm | POR | Quote |
4522 | Flat rotation specimen stage for 100 mm / 4" wafers, includes gearbox for increased coverage. Stage rotation speed variable between 8 and 20rpm | POR | Quote |
23850 | Tilt stage sub-assembly 4" | POR | Quote |
Carbon Supplies
4538 | Carbon fiber cord – high purity – 1m | POR | Quote |
4539 | Carbon fiber cord – high purity – 5m | POR | Quote |
4540 | Carbon fiber cord – standard grade – 1m | POR | Quote |
4541 | Carbon fiber cord – standard grade – 10m | POR | Quote |
4542 | Carbon fiber cord – standard grade – 100m | POR | Quote |
4543 | Carbon rods – 3.05 mm Ø x 50 mm length (shaped) pack of 10 | POR | Quote |
4544 | Carbon rods 3.05 mm Ø x 300 mm length (unshaped) pack of 10) | POR | Quote |
4546 | Manual rod shaper for 3.05 mm Ø carbon rods | POR | Quote |
12097 | Wedge Tool | POR | Quote |
Sputtering Targets
4523 | 57 mm Ø x 0.1 mm Gold | POR | Quote |
4524 | 57 mm Ø x 0.2 mm Gold | POR | Quote |
4525 | 57 mm Ø x 0.3 mm Gold | POR | Quote |
4526 | 57 mm Ø x 0.1 mm Gold/Palladium (80/20) | POR | Quote |
4527 | 57 mm Ø x 0.2 mm Gold/Palladium (80/20) | POR | Quote |
4528 | 57 mm Ø x 0.3 mm Gold/Palladium (80/20) | POR | Quote |
4529 | 57 mm Ø x 0.1 mm Platinum | POR | Quote |
4530 | 57 mm Ø x 0.2 mm Platinum | POR | Quote |
4531 | 57 mm Ø x 0.3 mm Platinum | POR | Quote |
4532 | 57 mm Ø x 0.1 mm Nickel | POR | Quote |
4533 | 57 mm Ø x 0.1 mm Silver | POR | Quote |
4534 | 57 mm Ø x 0.1 mm Palladium | POR | Quote |
4535 | 57 mm Ø x 0.1 mm Copper | POR | Quote |
4536 | 57 mm Ø x 0.1 mm Platinum/Palladium (80/20) | POR | Quote |
4537 | 57 mm Ø x 0.3 mm Platinum/Palladium (80/20) | POR | Quote |
Spare kits
4547 | Two-year spares kit for Q150R S Plus Includes: 57 mm Ø x 0.1 mm gold target, standard glass chamber assembly quartz crystals, O-rings |
POR | Quote |
4548 | Two-year spares kit for Q150R E Plus Includes: carbon fiber / cord, standard glass chamber assembly, quartz crystals, O-rings, springs |
POR | Quote |
4549 | Two-year spares kit for Q150R ES Plus Includes: 57 mm Ø x 0.1 mm gold target, carbon fiber / cord, standard glass chamber assembly, quartz crystals, O-rings, springs |
POR | Quote |
SEM/TEM Carbon Coaters Techniques and Applications
Sputter Coater Principles
Silver as a Removable Coating for Scanning Electron Microscopy